1-(2,4-Dichlorophenyl)-2-(1H-1,2,4-triazol-1-yl)ethanone → HCID 54073549, compound

HRID 1005448Notes

Reaction equation

HRID 1005448 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[C:9](=O)[CH2:10][N:11]1[CH:15]=[N:14][CH:13]=[N:12]1.[O:17]([CH:25]1[CH2:30][CH2:29][CH2:28][CH2:27][CH2:26]1)S(C(F)(F)F)(=O)=O>>[Cl:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[CH:9]=[C:10]([N:11]1[CH:15]=[N:14][CH:13]=[N:12]1)[O:17][CH:25]1[CH2:30][CH2:29][CH2:28][CH2:27][CH2:26]1

Participants

3

Reactant 2

HCID 7393741-(2,4-Dichlorophenyl)-2-(1H-1,2,4-triazol-1-yl)ethanoneHCID 14917491Cyclohexyl trifluoromethanesulfonate

Product 1

HCID 54073549HCID 54073549, compound

Procedure

Analogously to Example 1a,b, after reacting 1-(2,4-dichlorophenyl)-2-[1,2,4]triazol-1-yl-ethanone with cyclohexyl triflate there was obtained 1-[2-(2,4-dichloro-phenyl)-1-cyclohexyloxy-vinyl]-1H-[1,2,4]triazole as a white solid with m.p. 84° C.

Sources & evidence

ORD record
ord-f7943b887639465f8de3c69155a3bdd9
Source dataset
uspto-grants-2000_04
Patent number
US06054588

Reaction notes

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