HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-2-methylpropane → HCID 21700664, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-2-methylpropane | HCID 6555 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 565224 | HCID 565224 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 21700664 | HCID 21700664 | — |
Reaction Steps
The N-(2-furoyl)-2-methyl-3-nitroaniline (1 mmol) in DMSO was treated with potassium hydroxide (2.0 mmol) and 1-bromo-2-methylpropane (1.1 mmol) at 25° C. for 12 hr. Extraction and chromatography afforded N-(2-furoyl)-N-isobutyl-2-methyl-3-nitroaniline as a yellow syrup. TLC: Rf=0.40, 30% EtOAc-hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06054587 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-51ec494982ea45f3a217bdbe7e2691dd |
| Source note | uspto-grants-2000_04 |