HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodomethyl pivalate → HCID 53920308, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodomethyl pivalate | HCID 104401 | — |
| Reactant | HCID 86755354 | HCID 86755354 | — |
| Product | HCID 53920308 | HCID 53920308 | 84.5% |
Reaction Steps
The compound 76 (250 mg, 0.526 mmol) was converted to the ester with pivaloyloxymethyl iodide (140 mg, 0.578 mmol) under potassium carbonate (50.9 mg, 0.368 mmol) in the same manner as the example 61 to give the compound 78 (262 mg, 84%) as oil. Rf 0.18 (1:1 EtOAc - hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06054591 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-dfaf6ceb77aa4d97be94fc72f96a0b0c |
| Source note | uspto-grants-2000_04 |