HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbamate → HCID 69686723, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbamate | HCID 276 | — |
| Reactant | (5-(3,5-Dichlorophenylthio)-1-ethyl-4-isopropyl-1H-imidazol-2-yl)methanol | HCID 473933 | — |
| Reactant | HCID 18791977 | HCID 18791977 | — |
| Product | HCID 69686723 | HCID 69686723 | 71% |
Reaction Steps
The compound 19 (345 mg, 1.00 mmol) was converted to the carbamate with lauroyl isocyanate (5 eq.) in the same manner as the example 66 to give the compound 84 (430 mg, 71%) as crystals. Mp. 100-102° C. Rf 0.32 (1:2 EtOAc - hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06054591 |
| Source dataset | uspto-grants-2000_04 |
| ORD ID | ord-7283f16218694b28bf4af1d402f5e985 |
| Source note | uspto-grants-2000_04 |