HRID1005550

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID276

Carbamic acid, ion(1-)

CH2NO2-

结构：CCn1c(CO)nc(C(C)C)c1Sc1cc(Cl)cc(Cl)c1

HCID473933

(5-(3,5-Dichlorophenylthio)-1-ethyl-4-isopropyl-1H-imidazol-2-yl)methanol

C15H18Cl2N2OS

HCID10921144

4-chlorobenzoyl isocyanate

C8H4ClNO2

PRODUCTS

生成物

结构：CCn1c(COC(=O)NC(=O)c2ccc(Cl)cc2)nc(C(C)C)c1Sc1cc(Cl)cc(Cl)c1

HCID478190

未命名化合物

收率 25%

PROCEDURE

实验过程

The compound 19 (69 mg, 0.2 mmol) was converted to the carbamate with 4-chlorobenzoyl isocyanate (5 eq.) in the same manner as the example 66 to give the compound 86 (26 mg, 25%) as crystals. Mp. 82-83° C. Rf 0.13 (1:2 EtOAc - hexane).