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HRID1005551

反应详情

EQUATION

反应方程式

HRID 1005551 的结构方程式

REACTANTS

反应物

3
结构：NC(=O)[O-]
HCID276

Carbamic acid, ion(1-)

CH2NO2-

结构：CCn1c(CO)nc(C(C)C)c1Sc1cc(Cl)cc(Cl)c1
HCID473933

(5-(3,5-Dichlorophenylthio)-1-ethyl-4-isopropyl-1H-imidazol-2-yl)methanol

C15H18Cl2N2OS

结构：O=C=NC(=O)c1cc(Cl)cc(Cl)c1
HCID13513349

未命名化合物

PRODUCTS

生成物

1
结构：CCn1c(COC(=O)NC(=O)c2cc(Cl)cc(Cl)c2)nc(C(C)C)c1Sc1cc(Cl)cc(Cl)c1
HCID478191

未命名化合物

收率 78%

PROCEDURE

实验过程

The compound 19 (300 mg, 0.869 mmol) was converted to the carbamate with 3,5-dichlorobenzoyl isocyanate (1.5 eq.) in the same manner as the example 66 to give the compound 87 (380 mg, 78%) as crystals. Mp.124-125° C. Rf 0.23 (1:2 EtOAc-hexane)