HCID 22674365, compound → HCID 22674451, compound

Participants

Reaction Steps

A solution of 2-ethylthieno[3,2-d]pyrimidin-4-yl 2-thienylmethanone (170 mg, 0.6 mmol) in MeOH (10 mL) at room temperature was treated with NaBH (26 mg, 0.7 mmol), stirred for 1.5 h, concentrated in vacuo, treated with water (10 mL), extracted with EtOAc (2×10 mL) and purified by chromatography [SiO2; EtOAc] to give the title compound (109 mg, 64 %) as a pale yellow solid.

Provenance & Evidence