HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → 2-Benzyl benzylbromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | 2-Benzylbenzyl alcohol | HCID 74109 | — |
| Product | 2-Benzyl benzylbromide | HCID 12422098 | 98% |
Reaction Steps
2-Benzylbenzyl alcohol (commercial) (1 g) was suspended in 48% aqueous hydrobromic acid (10 ml) and stirred vigorously for 20 hours. The resultant suspended solid was extracted twice with hexane and the extracts dried (MgSO4) and evaporated to give 2-benzyl benzylbromide as yellow solid (1.3 g, 98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06787562B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-6a78670be9bd419cb9dfa46ff2da2c77 |
| Source note | uspto-grants-2004_09 |