HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl[(2-nitrophenyl)methyl]amine → N-ethyl-N-(2-aminobenzyl)amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl[(2-nitrophenyl)methyl]amine | HCID 14485081 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-ethyl-N-(2-aminobenzyl)amine | HCID 10329442 | 100% |
Reaction Steps
N-Ethyl-N-(2-nitrobenzyl)amine (4 g, 22 mmol) in ethanol (100 ml) was treated with 10% palladium-on-carbon (180 mg) and hydrogenated at N.T.P. for 2 hours. When uptake of hydrogen had ceased the reaction was filtered through Celite and evaporated to give N-ethyl-N-(2-aminobenzyl)amine (3.3 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06787562B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-be94a6d245f0490db1f74cfe4c69511f |
| Source note | uspto-grants-2004_09 |