HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxycyclopent-2-en-1-one → HCID 11183063, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxycyclopent-2-en-1-one | HCID 643476 | — |
| Reactant | HCID 178418865 | HCID 178418865 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 11183063 | HCID 11183063 | 94% |
Reaction Steps
The general procedure for the preparation of substrates using 3-methoxycyclopentenone (1.29 g, 11.5 mmol) and phenethylmagnesium chloride (23 mmol, 1M in THF) gave, after flash chromatography (4:1 hexanes:ethyl acetate), the title compound as a colorless liquid (2.01 g, 94%). Spectroscopic data were consistent with previously reported data for this compound.4
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06787655B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-99193911afa248078bc25bdf626ba25c |
| Source note | uspto-grants-2004_09 |