HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 11150959, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 11737800 | HCID 11737800 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 11150959 | HCID 11150959 | 100.3% |
Reaction Steps
2,4-Dichloro-3-(4,5-dihydro-4-methyl-5-oxo-1H-tetrazol-1-yl)benzoic acid (3.42 g) and thionylchloride (4.22 g) were added to 1,2-dichloroethane (50 ml). The mixture, after adding several drops of N,N-dimethylformamide, was refluxed upon heating for 4 hours. After cooling, the solvent was distilled off to obtain crude 2,4-dichloro-3-(4,5-dihydro-4-methyl-5-oxo-1H-tetrazol-1-yl)benzoyl chloride (3.65 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06790810B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-769fdd389ef944adac75bff553b9517e |
| Source note | uspto-grants-2004_09 |