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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1006474Generated: October 26, 2026

3-(Benzyloxy)-N-methoxy-N-methylbenzamide → 3-hydroxy-N-methoxy-N-methylbenzamide

https://huagongshe.com/reaction/1006474

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-(Benzyloxy)-N-methoxy-N-methylbenzamideHCID 21865361—
SolventTetrahydrofuranHCID 8028—
Product3-hydroxy-N-methoxy-N-methylbenzamideHCID 2186537698.4%

Reaction Steps

To a solution of 100 g (0.37 mol) B4 in 750 ml tetrahydrofurane 10 g Pd/C (10%) were added and the mixture was hydrogenated at atmospheric pressure for 2 hours. The catalyst war filtered off and the filtrate was evaporated to yield 66.0 g B5 (98%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06790852B2
Source datasetuspto-grants-2004_09
ORD IDord-d5323782eacd4e9eb1e6b03e295000c8
Source noteuspto-grants-2004_09