m-Chloroperbenzoic acid → HCID 69781579, compound

Participants

Reaction Steps

To a solution of 480 mg (1 mmol) E16.1 in 3 ml dichloromethane a solution of 246 mg (1 mmol) 3-chloroperbenzoic acid in 7 ml dichloromethane was added at 0° C. and stirred at this temperature for 6 hours. After washing with 5% aqueous sodium hydrogencarbonate and water (each 0° C.) the organic layer was dried over sodium sulfate and evaporated to dryness to yield 470 mg G16.1.1 (96%).

Provenance & Evidence