HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexyl isocyanate → Octylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexyl isocyanate | HCID 18502 | — |
| Reactant | Hydrogenated mdi | HCID 21202 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Octylamine | HCID 8143 | 220% |
Reaction Steps
According to the procedure described in Example 1, starting from 10 g (38.12 mmol) of methylene-bis(4-cyclohexylisocyanate), alias 4,4A′-methylene-bis(cyclohexyl isocyanate, into 200 ml of THF and 10.82 g (83.86 mmol) of octylamine into 100 ml of THF, 16.30 g of a white solid are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06790885B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-c3834f0705f643f18826c74abe6b1fd5 |
| Source note | uspto-grants-2004_09 |