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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1006552Generated: October 30, 2026

m-Chloroperbenzoic acid → HCID 22672113, compound

https://huagongshe.com/reaction/1006552

Reaction equation

Participants

RoleNameHCIDCharge
Reactantm-Chloroperbenzoic acidHCID 70297—
ReactantHCID 22671960HCID 22671960—
SolventDichloromethaneHCID 6344—
SolventEthyl AcetateHCID 8857—
ProductHCID 22672113HCID 22672113100.3%

Reaction Steps

To a solution of methyl 4-(2-cyclopentylsulfinylamino-5-trifluoromethylphenoxymethyl)benzoate (305 mg; prepared in Reference Example 33.) in methylene chloride (4.0 ml), meta-chloroperbenzoic acid (456 mg) was added at 0° C. The mixture was stirred for 1 hour. The reaction mixture was diluted with ethyl acetate, washed, dried over and concentrated under the reduced pressure to give the title compound (317 mg) having the following physical data.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06790866B2
Source datasetuspto-grants-2004_09
ORD IDord-8e4f78ce7e9f4a2f988a1a1e042762b3
Source noteuspto-grants-2004_09