HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylbutylamine → 8-bromo-N-butyl-N-methyl-octanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylbutylamine | HCID 8068 | — |
| Reactant | 8-Bromooctanoic acid | HCID 548275 | — |
| Product | 8-bromo-N-butyl-N-methyl-octanamide | HCID 22672743 | — |
Reaction Steps
Using the procedure of Step A of Example 3, 5 g of 8-bromo octanoic acid and 13 ml of N-methyl butylamine were reacted to obtain after chromatography on silica (eluant: methylene chloride-acetone 95-5), 6.14 g of the expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06790971B1 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-25f0ff04db93408d8d29067dd3f954b3 |
| Source note | uspto-grants-2004_09 |