N-Methylbutylamine → 6-Bromo-N-butyl-N-methylhexanamide

HRID 1006752Notes

Reaction equation

HRID 1006752 reaction equation
[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][C:7]([OH:9])=O.[CH3:10][NH:11][CH2:12][CH2:13][CH2:14][CH3:15]>>[Br:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][C:7]([N:11]([CH2:12][CH2:13][CH2:14][CH3:15])[CH3:10])=[O:9]

Participants

3

Reactant 2

HCID 8068N-MethylbutylamineHCID 202106-Bromohexanoic acid

Product 1

HCID 226727536-Bromo-N-butyl-N-methylhexanamide

Procedure

Using the procedure of Step A of Example 3, 4 88 g of 6-bromohexanoic acid and 4.36 ml of N-methylbutylamine were reacted to obtain 7. g of the expected product which was used as is for the following step.

Workup

  1. customwere reacted
  2. customto obtain 7

Sources & evidence

ORD record
ord-0092dfc84e9549e5b04b49a88ace5dd0
Source dataset
uspto-grants-2004_09
Patent number
US06790971B1

Reaction notes

Loading…