HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 69431418, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 69430258 | HCID 69430258 | — |
| Product | HCID 69431418 | HCID 69431418 | 60.8% |
Reaction Steps
(3SR,5RS)-5-Benzyloxymethyl-1-(naphthalene-2-sulfonyl)-piperidine-3-carboxylic acid methyl ester (2.70 g) was reduced with lithium aluminium hydride as described in Example 17 to obtain (3SR,5RS)-[5-benzyloxymethyl-1-(naphthalene-2-sulfonyl)-piperidin-3-yl]-methanol (1.54 g) as a syrup, MS: 426 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06790860B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-52741407128249ab85468f4ca326ef86 |
| Source note | uspto-grants-2004_09 |