HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 22503052, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | 4-Methoxybenzonitrile | HCID 70129 | — |
| Reactant | HCID 22502967 | HCID 22502967 | — |
| Product | HCID 22503052 | HCID 22503052 | — |
Reaction Steps
6-Methoxy-3-(4-methoxyphenyl)isoquinolin-1-one (0.40 g) obtained by reacting N-methyl-4-methoxy-2-methylbenzamide (1.0 g) and 4-methoxybenzonitrile (0.75 g) according to Example 10-1 was reacted with phosphorus oxychloride (10 ml) according to Example 10-2, to give 1-chloro-6-methoxy-3-(4-methoxyphenyl)isoquinoline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06790844B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-e48dd52d46ba465f9edba9d0348250e0 |
| Source note | uspto-grants-2004_09 |