Pyridine → HCID 54337256, compound

Participants

Reaction Steps

To a solution of 53.5 g of stearylamine and 15.7 g of pyridine in 599.2 g of tetrahydrofuran was added under room temperature a solution of 12.0 g of oxalyl chloride in 120.0 g of tetrahydrofuran dropwise. After stirring, the mixture was stirred at room temperature for 5 hours. The deposited crystal was filtrated, washed with water and re-crystallized from toluene, to obtain 19.6 g of the intended compound.

Provenance & Evidence