HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyanopyridine → HCID 10130981, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyanopyridine | HCID 7506 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Benzoic acid, 2-mercapto-, methyl ester | HCID 21009 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 10130981 | HCID 10130981 | 30.7% |
Reaction Steps
Methyl thiosalicylate (2.0 g, 11.9 mM) and 4-cyanopyridine (1.2 g, 11.5 mM) were dissolved in toluene (5 ml), and then triethylamine (2 ml) was added thereto. After heating the mixture under reflux for 22 hours, the same processes as described in Reference Example 1 were performed to give the title compound as crystals (850 mg, 30.7%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06794383B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-b3da852df2ea43eaac75a5c81d70e186 |
| Source note | uspto-grants-2004_09 |