4-Methoxy-2-nitroaniline → HCID 9966358, compound

HRID 1007183Notes

Reaction equation

HRID 1007183 reaction equation
[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](Cl)=[O:7])=[CH:4][N:3]=1.[CH3:11][O:12][C:13]1[CH:19]=[CH:18][C:16]([NH2:17])=[C:15]([N+:20]([O-:22])=[O:21])[CH:14]=1>>[Cl:1][C:2]1[N:3]=[CH:4][C:5]([C:6]([NH:17][C:16]2[CH:18]=[CH:19][C:13]([O:12][CH3:11])=[CH:14][C:15]=2[N+:20]([O-:22])=[O:21])=[O:7])=[CH:9][CH:10]=1

Participants

3

Reactant 2

HCID 667934-Methoxy-2-nitroanilineHCID 27821656-Chloronicotinoyl Chloride

Product 1

HCID 9966358HCID 9966358, compound

Procedure

The title compound was prepared from 6-chloronicotinoyl chloride and 4-methoxy-2-nitroaniline and was obtained as a yellow solid as described in Example 1. 1H NMR (CDCl3): 11.13 (s, 1H), 9.01 (d, J=2.7, 1H), 8.83 (d, J=9.3, 1H), 8.24-8.20 (m, 1H), 7.76 (d, J=2.7, 1H), 7.52 (d, J=8.7, 1H), 7.35-7.31 (m, 1H), 3.90 (s, 3H).

Workup

  1. customwas obtained as a yellow solid

Sources & evidence

ORD record
ord-5008c920e7ca45609913a0e6173bee7b
Source dataset
uspto-grants-2004_09
Patent number
US06794397B2

Reaction notes

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