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HRID1007185

反应详情

EQUATION

反应方程式

HRID 1007185 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(N)c([N+](=O)[O-])c1
HCID6978

4-Methyl-2-nitroaniline

C7H8N2O2

结构：O=C(Cl)c1ccc(Cl)nc1
HCID2782165

6-Chloropyridine-3-carbonyl chloride

C6H3Cl2NO

PRODUCTS

生成物

1
结构：Cc1ccc(NC(=O)c2ccc(Cl)nc2)c([N+](=O)[O-])c1
HCID9814567

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 6-chloronicotinoyl chloride and 4-methyl-2-nitroaniline and was obtained as a yellow solid as described in Example 1. 1H NMR (CDCl3): 11.29 (s, 1H), 9.02 (d, J=2.7, 1H), 8.81 (d, J=8.7, 1H), 8.24-8.21 (m, 1H), 8.11 (s, 1H), 7.58-7.50 (m, 2H), 2.44 (s, 3H).

WORKUP

后处理

  1. customwas obtained as a yellow solid