2-Nitroaniline → HCID 22668929, compound

HRID 1007186Notes

Reaction equation

HRID 1007186 reaction equation
[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](Cl)=[O:7])=[CH:4][N:3]=1.[N+:11]([C:14]1[CH:20]=[CH:19][CH:18]=[CH:17][C:15]=1[NH2:16])([O-:13])=[O:12]>>[Cl:1][C:2]1[N:3]=[CH:4][C:5]([C:6]([NH:16][C:15]2[CH:17]=[CH:18][CH:19]=[CH:20][C:14]=2[N+:11]([O-:13])=[O:12])=[O:7])=[CH:9][CH:10]=1

Participants

3

Reactant 2

HCID 69462-NitroanilineHCID 27821656-Chloronicotinoyl Chloride

Product 1

HCID 22668929HCID 22668929, compound

Procedure

The title compound was prepared from 6-chloronicotinoyl chloride and 2-nitroaniline and was obtained as a yellow solid as described in Example 1. 1H NMR (CDCl3): 10.99 (s, 1H), 8.95-8.94 (m, 1H), 8.36-8.33 (m, 1H), 8.02-7.99 (m, 1H), 7.80-7.69 (m, 3H), 7.48-7.42 (m, 1H).

Workup

  1. customwas obtained as a yellow solid

Sources & evidence

ORD record
ord-fa8a84a3066246e5acb6f550b15ebc24
Source dataset
uspto-grants-2004_09
Patent number
US06794397B2

Reaction notes

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