4-Methoxy-2-nitroaniline → HCID 22668932, compound

HRID 1007188Notes

Reaction equation

HRID 1007188 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([C:8](Cl)=[O:9])[CH:5]=[C:4]([Cl:11])[N:3]=1.[CH3:12][O:13][C:14]1[CH:20]=[CH:19][C:17]([NH2:18])=[C:16]([N+:21]([O-:23])=[O:22])[CH:15]=1>>[Cl:1][C:2]1[CH:7]=[C:6]([C:8]([NH:18][C:17]2[CH:19]=[CH:20][C:14]([O:13][CH3:12])=[CH:15][C:16]=2[N+:21]([O-:23])=[O:22])=[O:9])[CH:5]=[C:4]([Cl:11])[N:3]=1

Participants

3

Reactant 2

HCID 667934-Methoxy-2-nitroanilineHCID 27816432,6-Dichloro-isonicotinoyl chloride

Product 1

HCID 22668932HCID 22668932, compound

Procedure

The title compound was prepared from 2,6-dichloropyridine-4-carbonyl chloride and 4-methoxy-2-nitroaniline and was obtained as a yellow solid as described in Example 1. 1H NMR (CDCl3): 11.12 (s, 1H), 8.78 (d, J=9.3, 1H), 7.77 (d, J=3.0, 1H), 7.75 (s, 2H), 7.35-7.31 (m, 1H), 3.91 (s, 3H).

Workup

  1. customwas obtained as a yellow solid

Sources & evidence

ORD record
ord-84c76e3368ff40ceabfe26b0e930c812
Source dataset
uspto-grants-2004_09
Patent number
US06794397B2

Reaction notes

Loading…