4-Methoxy-2-nitroaniline → HCID 2789565, compound

HRID 1007190Notes

Reaction equation

HRID 1007190 reaction equation
[C:1](Cl)(=[O:8])[C:2]1[CH:7]=[CH:6][N:5]=[CH:4][CH:3]=1.[CH3:10][O:11][C:12]1[CH:18]=[CH:17][C:15]([NH2:16])=[C:14]([N+:19]([O-:21])=[O:20])[CH:13]=1>>[CH3:10][O:11][C:12]1[CH:18]=[CH:17][C:15]([NH:16][C:1]([C:2]2[CH:7]=[CH:6][N:5]=[CH:4][CH:3]=2)=[O:8])=[C:14]([N+:19]([O-:21])=[O:20])[CH:13]=1

Participants

3

Reactant 2

HCID 667934-Methoxy-2-nitroanilineHCID 417436Pyridine-4-carbonyl chloride

Product 1

HCID 2789565HCID 2789565, compound

Procedure

The title compound was prepared from isonicotinoyl chloride and 4-methoxy-2-nitroaniline and was obtained as an orange yellow solid as described in Example 1. 1H NMR (CDCl3): 10.79 (s, 1H), 8.83-8.81 (m, 2H), 7.85-7.83 (m, 2H), 7.61-7.55 (m, 2H), 7.40-7.36 (m, 1H), 3.87 (s, 3H).

Workup

  1. customwas obtained as an orange yellow solid

Sources & evidence

ORD record
ord-1142c679e2864ad787e6277c1269103f
Source dataset
uspto-grants-2004_09
Patent number
US06794397B2

Reaction notes

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