4-Methoxy-2-nitroaniline → HCID 9902590, compound

HRID 1007192Notes

Reaction equation

HRID 1007192 reaction equation
[Cl:1][C:2]1[C:3]([Cl:11])=[N:4][CH:5]=[C:6]([CH:10]=1)[C:7]([OH:9])=O.[CH3:12][O:13][C:14]1[CH:20]=[CH:19][C:17]([NH2:18])=[C:16]([N+:21]([O-:23])=[O:22])[CH:15]=1>>[Cl:1][C:2]1[CH:10]=[C:6]([C:7]([NH:18][C:17]2[CH:19]=[CH:20][C:14]([O:13][CH3:12])=[CH:15][C:16]=2[N+:21]([O-:23])=[O:22])=[O:9])[CH:5]=[N:4][C:3]=1[Cl:11]

Participants

3

Reactant 2

HCID 667934-Methoxy-2-nitroanilineHCID 2479875,6-Dichloronicotinic acid

Product 1

HCID 9902590HCID 9902590, compound

Procedure

The title compound was prepared from 5,6-dichloronicotinic acid and 4-methoxy-2-nitroaniline and was obtained as a yellow solid as described in Example 15. 1H NMR (DMSO-d6): 10.85 (bs, 1H), 8.88 (d, J=2.4, 1H), 8.59 (d, J=2.4, 1H), 7.58-7.54 (m, 2H), 7.39-7.35 (m, 1H), 3.87 (s, 3H).

Workup

  1. customwas obtained as a yellow solid

Sources & evidence

ORD record
ord-c85bc233da514fa48c9c370f00883357
Source dataset
uspto-grants-2004_09
Patent number
US06794397B2

Reaction notes

Loading…