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HRID1007201

反应详情

EQUATION

反应方程式

HRID 1007201 的结构方程式

REACTANTS

反应物

2
结构：CCOc1ccc(N)c([N+](=O)[O-])c1
HCID69229

4-Ethoxy-2-nitroaniline

C8H10N2O3

结构：Cc1ccc(C(=O)O)cn1
HCID137860

6-Methylnicotinic acid

C7H7NO2

PRODUCTS

生成物

1
结构：CCOc1ccc(NC(=O)c2ccc(C)nc2)c([N+](=O)[O-])c1
HCID9817832

N-(4-Ethoxy-2-nitrophenyl)-6-methylpyridine-3-carboxamide

C15H15N3O4

PROCEDURE

实验过程

The title compound was prepared from 6-methylnicotinic acid and 4-ethoxy-2-nitroaniline and was obtained as a yellow solid as described in Example 15. 1H NMR (CDCl3): 11.09 (s, 1H), 9.12 (d, J=2.1, 1H), 8.85 (d, J=9.3, 1H), 8.16-8.13 (m, 1H), 7.73 (d, J=3.0, 1H), 7.34-7.29 (m, 2H), 4.11 (q, J=6.9, 2H), 2.67 (s, 3H), 1.46 (t, J=6.9, 3H).

WORKUP

后处理

  1. customwas obtained as a yellow solid