4,5-Dimethyl-2-nitrobenzenamine → HCID 22668928, compound

HRID 1007202Notes

Reaction equation

HRID 1007202 reaction equation
[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](Cl)=[O:7])=[CH:4][N:3]=1.[CH3:11][C:12]1[C:18]([CH3:19])=[CH:17][C:15]([NH2:16])=[C:14]([N+:20]([O-:22])=[O:21])[CH:13]=1>>[Cl:1][C:2]1[N:3]=[CH:4][C:5]([C:6]([NH:16][C:15]2[CH:17]=[C:18]([CH3:19])[C:12]([CH3:11])=[CH:13][C:14]=2[N+:20]([O-:22])=[O:21])=[O:7])=[CH:9][CH:10]=1

Participants

3

Reactant 2

HCID 814454,5-Dimethyl-2-nitrobenzenamineHCID 27821656-Chloronicotinoyl Chloride

Product 1

HCID 22668928HCID 22668928, compound

Procedure

The title compound was prepared from 6-chloronicotinoyl chloride and 4,5-dimethyl-2-nitroaniline and was obtained as an orange solid as described in Example 1. 1H NMR (CDCl3): 11.38 (s, 1H), 9.03 (d, J=2.1, 1H), 8.72 (s, 1H), 8.24-8.21 (m, 1H), 8.07 (s, 1H), 7.52 (d, J=8.7, 1H), 2.41 (s, 3H), 2.34 (s, 3H).

Workup

  1. customwas obtained as an orange solid

Sources & evidence

ORD record
ord-c24b186149f74e00b544d76d0ae5609a
Source dataset
uspto-grants-2004_09
Patent number
US06794397B2

Reaction notes

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