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HRID1007202

反应详情

EQUATION

反应方程式

HRID 1007202 的结构方程式

REACTANTS

反应物

2
结构：Cc1cc(N)c([N+](=O)[O-])cc1C
HCID81445

4,5-Dimethyl-2-nitroaniline

C8H10N2O2

结构：O=C(Cl)c1ccc(Cl)nc1
HCID2782165

6-Chloropyridine-3-carbonyl chloride

C6H3Cl2NO

PRODUCTS

生成物

1
结构：Cc1cc(NC(=O)c2ccc(Cl)nc2)c([N+](=O)[O-])cc1C
HCID22668928

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 6-chloronicotinoyl chloride and 4,5-dimethyl-2-nitroaniline and was obtained as an orange solid as described in Example 1. 1H NMR (CDCl3): 11.38 (s, 1H), 9.03 (d, J=2.1, 1H), 8.72 (s, 1H), 8.24-8.21 (m, 1H), 8.07 (s, 1H), 7.52 (d, J=8.7, 1H), 2.41 (s, 3H), 2.34 (s, 3H).

WORKUP

后处理

  1. customwas obtained as an orange solid