4-Methoxy-2-nitroaniline → HCID 2843300, compound

HRID 1007203Notes

Reaction equation

HRID 1007203 reaction equation
[C:1](Cl)(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[N:4][CH:3]=1.[CH3:10][O:11][C:12]1[CH:18]=[CH:17][C:15]([NH2:16])=[C:14]([N+:19]([O-:21])=[O:20])[CH:13]=1>>[CH3:10][O:11][C:12]1[CH:18]=[CH:17][C:15]([NH:16][C:1]([C:2]2[CH:3]=[N:4][CH:5]=[CH:6][CH:7]=2)=[O:8])=[C:14]([N+:19]([O-:21])=[O:20])[CH:13]=1

Participants

3

Reactant 2

HCID 667934-Methoxy-2-nitroanilineHCID 82604Nicotinoyl chloride

Product 1

HCID 2843300HCID 2843300, compound

Procedure

The title compound was prepared from nicotinoyl chloride and 4-methoxy-2-nitroaniline and was obtained as an orange solid as described in Example 1. 1H NMR (DMSO-d6): 10.74 (s, 1H), 9.10 (d, J=2.4, 1H), 8.80-8.78 (m, 1H), 7.62-7.54 (m, 3H), 7.39-7.35 (m, 1H), 3.87 (s, 3H).

Workup

  1. customwas obtained as an orange solid

Sources & evidence

ORD record
ord-5054b093b3294b349fa9c547bc5cff1c
Source dataset
uspto-grants-2004_09
Patent number
US06794397B2

Reaction notes

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