HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethoxy-2-nitroaniline → 6-(2,2,2-Triflouroethoxy)-N-(4ethoxy-2-nitrophenyl)-3-pyridinecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethoxy-2-nitroaniline | HCID 69229 | — |
| Reactant | 6-(2,2,2-Trifluoroethoxy)pyridine-3-carboxylic acid | HCID 2781028 | — |
| Product | 6-(2,2,2-Triflouroethoxy)-N-(4ethoxy-2-nitrophenyl)-3-pyridinecarboxamide | HCID 22668923 | — |
Reaction Steps
The title compound was prepared from 6-(2,2,2-trifluoroethoxy)pyridine-3-carboxylic acid and 4-ethoxy-2-nitroaniline as a yellow solid as described in Example 15. 1H NMR (CDCl3): 11.05 (s, 1H), 8.84-8.80 (m, 2H), 8.25-8.21 (m, 1H), 7.73 (d, J=3.0, 1H), 7.32-7.28 (m, 1H), 7.01 (d, J=8.7, 1H), 4.86 (q, J=8.4, 2H), 4.11 (q, J=6.9, 2H), 1.46 (t, J=6.9, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06794397B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-e6ab116cef3e4cb09e6b6420f5aeb9ee |
| Source note | uspto-grants-2004_09 |