4-Methoxy-2,3-dinitroaniline → HCID 22668936, compound

HRID 1007220Notes

Reaction equation

HRID 1007220 reaction equation
[Cl:1][C:2]1[CH:10]=[CH:9][C:5]([C:6](Cl)=[O:7])=[CH:4][N:3]=1.[N+:11]([C:14]1[C:20]([N+:21]([O-:23])=[O:22])=[C:19]([O:24][CH3:25])[CH:18]=[CH:17][C:15]=1[NH2:16])([O-:13])=[O:12]>>[Cl:1][C:2]1[N:3]=[CH:4][C:5]([C:6]([NH:16][C:15]2[CH:17]=[CH:18][C:19]([O:24][CH3:25])=[C:20]([N+:21]([O-:23])=[O:22])[C:14]=2[N+:11]([O-:13])=[O:12])=[O:7])=[CH:9][CH:10]=1

Participants

3

Reactant 2

HCID 2322694-Methoxy-2,3-dinitroanilineHCID 27821656-Chloronicotinoyl Chloride

Product 1

HCID 22668936HCID 22668936, compound

Procedure

The title compound was prepared from 6-chloronicotinoyl chloride and 2,3-dinitro-4-methoxyaniline as a white solid as described in Example 1. 1H NMR (CDCl3): 9.99 (s, 1H), 8.96 (d, J=2.4, 1H), 8.77 (d, J=9.3, 1H), 8.18-8.14 (m, 1H), 7.53 (d, J=9.0, 1H), 7.45 (d, J=9.3, 1H), 4.02 (s, 3H).

Sources & evidence

ORD record
ord-fe914f803f6a4815b3e2ad1bc292cb67
Source dataset
uspto-grants-2004_09
Patent number
US06794397B2

Reaction notes

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