Trifluoroacetic acid → HCID 178511553, compound

Participants

Reaction Steps

A solution of 0.53 g of cis-N-(tert-butoxycarbonyl)-4-trifluoroacetylaminomethylcyclohexylamine in methylene chloride was combined with 2 mL of trifluoroacetic acid, and stirred for 2 hours. The reaction solution was basified by addition of a saturated solution of sodium hydrogen carbonate, and then extracted with chloroform. After drying over sodium sulfate, 0.19 g of the desirable compound was obtained as a pale yellow oil.

Provenance & Evidence