HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridinium chloride → 6-Chloro-2-(3-fluoro-4-hydroxyphenyl)benzo[d]oxazol-5-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridinium chloride | HCID 10176127 | — |
| Reactant | N-(4-Chloro-2,5-dihydroxyphenyl)-3-fluoro-4-hydroxybenzamide | HCID 21907381 | — |
| Product | 6-Chloro-2-(3-fluoro-4-hydroxyphenyl)benzo[d]oxazol-5-ol | HCID 135493223 | — |
Reaction Steps
The title compound was prepared in substantially the same manner as described in Example 1, step b, from N-(4-chloro-2,5-dihydroxyphenyl)-3-fluoro-4-hydroxybenzamide and pyridine hydrochloride and was obtained as a white solid, m.p. 258-260° C.; MS m/e 278 (M−H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06794403B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-86088c20403149d7ae34d1b4694c9419 |
| Source note | uspto-grants-2004_09 |