(1,3-Dithiolan-4-yl)methanol → HCID 22670133, compound

HRID 1007517Notes

Reaction equation

HRID 1007517 reaction equation
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH:11]1[S:15][CH:14]([CH2:16]O)[CH2:13][S:12]1.OCC1CSC[S:21]1>>[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][C:2]=1[CH:11]1[S:15][CH:14]([CH2:16][SH:21])[CH2:13][S:12]1

Participants

3

Reactant 2

HCID 22147(1,3-Dithiolan-4-yl)methanolHCID 22670183HCID 22670183, compound

Product 1

HCID 22670133HCID 22670133, compound

Procedure

The same method was followed as in Example 1 except that 2-(β-naphtyl)-4-hydroxymethyl-1,3-dithiolane produced in Example 4 was used in stead of 4-hydroxymethyl-1,3-dithiolane synthesized in Manufacturing Example 1 to obtain 2-(β-naphtyl)-4-mercaptomethyl-1,3-dithiolane represented by the following formula (2-8).

Workup

  1. customsynthesized in Manufacturing Example 1

Sources & evidence

ORD record
ord-dc24b683d7f7481c86433eb27160b47d
Source dataset
uspto-grants-2004_09
Patent number
US06794471B2

Reaction notes

Loading…