(1,3-Dithiolan-4-yl)methanol → HCID 22670087, compound

HRID 1007518Notes

Reaction equation

HRID 1007518 reaction equation
[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]1[S:10][CH:9]([CH2:11]O)[CH2:8][S:7]1.OCC1CSC[S:16]1>>[S:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]1[S:10][CH:9]([CH2:11][SH:16])[CH2:8][S:7]1

Participants

3

Reactant 2

HCID 22147(1,3-Dithiolan-4-yl)methanolHCID 22670290HCID 22670290, compound

Product 1

HCID 22670087HCID 22670087, compound

Procedure

The same method was followed as in Example 1 except that 2-(thiophen-2-yl)-4-hydroxymethyl-1,3-dithiolane produced in Example 5 was used in stead of 4-hydroxymethyl-1,3-dithiolane synthesized in Manufacturing Example 1 to obtain 2-(thiophen-2-yl)-4-mercaptomethyl-1,3-dithiolane represented by the following formula (2-9).

Workup

  1. customsynthesized in Manufacturing Example 1

Sources & evidence

ORD record
ord-d7e39805fa7443478b9515114ce02fba
Source dataset
uspto-grants-2004_09
Patent number
US06794471B2

Reaction notes

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