Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Hexafluoroacetone trihydrate | HCID 36719 | — |
| Product | Hexafluoroacetone | HCID 12695 | — |
Reaction Steps
The compound was prepared in analogy to W. Steglich et al., Chem. Ber., 107:1488-1498 (1974). Anhydrous hexafluoroacetone (HFA) was prepared by adding HFA trihydrate dropwise to concentrated sulfuric acid heated to 80° C. The resulting gas was once more washed with concentrated sulfuric acid and then passed into the gas space of the reaction flask. A reflux condenser packed with acetone/dry ice was fitted on the gas outlet of the flask.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06794517B2 |
|---|
| Source dataset | uspto-grants-2004_09 |
|---|
| ORD ID | ord-822d19d7e6bd4489be05babef95f12e7 |
|---|
| Source note | uspto-grants-2004_09 |
|---|
