huagongshe.com
HRID1007615

反应详情

EQUATION

反应方程式

HRID 1007615 的结构方程式

REACTANTS

反应物

1
结构：CC1(C)OCC(C2OC3OC(C)(C)OC3C2OCc2ccccc2)O1
HCID97907

未命名化合物

PRODUCTS

生成物

1
结构：CC1(C)O[C@H]2O[C@H]([C@H](O)CO)[C@H](OCc3ccccc3)[C@H]2O1
HCID11088188

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

Partial hydrolysis of 30B (50 g) was achieved in 75% acetic acid in a period of 20 h. Concentration to a smaller volume and extraction with ethyl acetate yielded 30C, 40 g, (90%). Homogeneous by TLC.

WORKUP

后处理

  1. concentrationConcentration
  2. extractionto a smaller volume and extraction with ethyl acetate