HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1007664Generated: October 29, 2026
Methacrolein → 2-Methyl-3-(phenylsulfanyl)propanal
https://huagongshe.com/reaction/1007664
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methacrolein | HCID 6562 | — |
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Product | 2-Methyl-3-(phenylsulfanyl)propanal | HCID 11073998 | — |
Reaction Steps
To a stirred mixture of 51.4 g (0.733 mole) of methacrolein and 2 g (0.018 mole) of triethylamine at 0-5° C. is added 80.8 g (0.733 mole) of benzenethiol slowly. The addition rate is such that the temperature was under 10° C. The reaction mixture is stirred at 0-5° C. for one hour. The mixture is placed on a rotary evaporator to remove triethylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06794544B2 |
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| Source dataset | uspto-grants-2004_09 |
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| ORD ID | ord-74042e6dbaca4d2ab0e7d7381fb1930e |
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| Source note | uspto-grants-2004_09 |
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