Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | Lithium Chloride | HCID 433294 | — |
| Reactant | 3-Cyanophenylalanine | HCID 2734509 | — |
| Solvent | 1-Methoxyethanol | HCID 3015637 | — |
| Product | HCID 178511771 | HCID 178511771 | 200.8% |
Reaction Steps
A suspension of L-3-cyano-phenylalanine (0.150 g, 0.79 mmol), lithium chloride (0.060 g, 1.43 mmol) and sodium azide (0.067 g, 1.03 mmol) in methoxyethanol (500 μL) was heated at 125° C. for 18 h. The solvent was evaporated to yield 370 mg of crude 3-tetrazolyl-L-phenylalanine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06794404B2 |
|---|
| Source dataset | uspto-grants-2004_09 |
|---|
| ORD ID | ord-504e601c4af24de2adf2b402e3cf4305 |
|---|
| Source note | uspto-grants-2004_09 |
|---|
