HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Toluidine → HCID 15545981, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Toluidine | HCID 7934 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 3,5-Dichloropyrazine-2-carboxamide | HCID 22665521 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 15545981 | HCID 15545981 | — |
Reaction Steps
To an acetonitrile solution of 3,5-dichloropyrazine-2-carboxamide were added 3-methylaniline and N,N-diisopropylethylamine, followed by heating to reflux for 17 hours. Thereafter, purification in the usual way afforded 5-chloro-3-(3-methylanilino)pyrazine-2-carboxamide (yellow solid).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06797706B1 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-d9bc789e653f468d997e7abdfac30adc |
| Source note | uspto-grants-2004_09 |