HuagongsheHuagongshe Chemistry Print Report · For research reference only
5,5-Diphenylpenta-2,4-dienoic acid → 5,5-diphenylpentanoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5,5-Diphenylpenta-2,4-dienoic acid | HCID 54410079 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 5,5-diphenylpentanoic Acid | HCID 10999607 | 97.3% |
Reaction Steps
5,5-Diphenylpenta-2,4-dienoic acid (0.90 g) was dispersed in methanol (15 mL), and 5% palladium-carbon (90 mg) was added thereto. The mixture was subjected to catalytic reduction for two hours under hydrogen. The insoluble matter was separated through filtration and washed with methanol. The filtrate was subjected to distillation under reduced pressure, to thereby yield 0.89 g of the product of interest (yield 97.3%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06797711B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-29479d58ce1740898150a170206f3cb6 |
| Source note | uspto-grants-2004_09 |