Oxalic Acid → HCID 9844758, compound

Participants

Reaction Steps

In 20 mL of ethyl acetate is dissolved 2.03 g of N-[2-(2-benzo[b]thiophen-5-ylethoxy)ethyl]-N-benzyl-N-methylamine. After adding 10 mL of a solution of 0.65 g of oxalic acid in ethyl acetate to the solution the resulting mixture is stirred at ambient temperature for 2 hours. The deposited crystal is collected by filtration, washed with ethyl acetate and dried to obtain 1.98 g of N-[2-(2-benzo[b]thiophen-5-ylethoxy)ethyl]-N-benzyl-N-methylamine oxalate.

Provenance & Evidence