HRID1008037

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CN(C)c1ccc(N=Nc2ccc(S(=O)(=O)Cl)cc2)cc1

HCID91660

Benzenesulfonyl chloride, 4-[2-[4-(dimethylamino)phenyl]diazenyl]-

C14H14ClN3O2S

HCID21913053

未命名化合物

PRODUCTS

生成物

结构：Cc1nc(N)c2nc(C)n(CCOCCNS(=O)(=O)c3ccc(N=Nc4ccc(N(C)C)cc4)cc3)c2c1C

HCID10437562

未命名化合物

PROCEDURE

实验过程

Using the method of Examples 34-50, 4-dimethylaminoazobenzene-4′-sulfonyl chloride was reacted with 1-[2-(2-aminoethoxy)ethyl]-2,6,7-trimethyl-1H-imidazo[4,5-c]pyridin-4-amine to provide the desired compound. The product was purified using Method A. The observed accurate mass was 551.2551.

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-ed438f9a29814fdc884b2a8488d2fbd9
来源数据集: uspto-grants-2004_09
DOI: 10.6084/m9.figshare.5104873.v1
专利: US06797718B2
来源说明: uspto-grants-2004_09

反应 SMILES

[CH3:1][N:2]([C:4]1[CH:9]=[CH:8][C:7]([N:10]=[N:11][C:12]2[CH:17]=[CH:16][C:15]([S:18](Cl)(=[O:20])=[O:19])=[CH:14][CH:13]=2)=[CH:6][CH:5]=1)[CH3:3].[NH2:22][CH2:23][CH2:24][O:25][CH2:26][CH2:27][N:28]1[C:36]2[C:35]([CH3:37])=[C:34]([CH3:38])[N:33]=[C:32]([NH2:39])[C:31]=2[N:30]=[C:29]1[CH3:40]>>[NH2:39][C:32]1[C:31]2[N:30]=[C:29]([CH3:40])[N:28]([CH2:27][CH2:26][O:25][CH2:24][CH2:23][NH:22][S:18]([C:15]3[CH:16]=[CH:17][C:12]([N:11]=[N:10][C:7]4[CH:8]=[CH:9][C:4]([N:2]([CH3:3])[CH3:1])=[CH:5][CH:6]=4)=[CH:13][CH:14]=3)(=[O:20])=[O:19])[C:36]=2[C:35]([CH3:37])=[C:34]([CH3:38])[N:33]=1