HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Amino-1-hexanol → HCID 21913650, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Amino-1-hexanol | HCID 19960 | — |
| Reactant | 2,4-Dichloro-5,6-dimethyl-3-nitropyridine | HCID 12109123 | — |
| Product | HCID 21913650 | HCID 21913650 | 36.1% |
Reaction Steps
Using the general method of Example 89 Part A, 6-aminohexan-1-ol (15.91 g, 135.7 mmol) was reacted with 2,4-dichloro-5,6-dimethyl-3-nitropyridine (30 g, 136 mmol) to provide 14.79 g of 6-[(2-chloro-5,6-dimethyl-3-nitropyridin-4-yl)amino]hexan-1-ol as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06797718B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-31c86d9941dd4e79a3c50b8cad5238d3 |
| Source note | uspto-grants-2004_09 |