HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 69352948, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 2,4-Difluorophenyl isocyanate | HCID 593258 | — |
| Reactant | 4-[(6,7-Dimethoxy-4-quinolyl)oxy]-2,3-dimethylaniline | HCID 21890439 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 69352948 | HCID 69352948 | 70% |
Reaction Steps
4-[(6,7-Dimethoxy-4-quinolyl)oxy]-2,3-dimethyl-aniline (710 mg) was dissolved in chloroform (7 ml), and 2,4-difluorophenyl isocyanate (310 μl) was then added to the solution. The mixture was heated under reflux for one hr, and a large amount of ether was added to the reaction solution. The resultant precipitate was collected by suction filtration to give 735 mg (yield 70%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06797823B1 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-937f4bca62984b35b814bd0e732b516b |
| Source note | uspto-grants-2004_09 |