HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Difluorophenyl isocyanate → HCID 22667079, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Difluorophenyl isocyanate | HCID 593258 | — |
| Reactant | HCID 22667151 | HCID 22667151 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 22667079 | HCID 22667079 | — |
Reaction Steps
4-[(6,7-Dimethoxy-4-quinazolinyl)oxy]-2-methyl-aniline (50 mg) was dissolved in chloroform (3 ml), and 2,4-difluorophenyl isocyanate (23 μl) was then added to the solution. The mixture was heated under reflux overnight. The precipitated crystal was collected by filtration and was washed to quantitatively give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06797823B1 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-52042e5c740649b5bf4a46c402ff86b0 |
| Source note | uspto-grants-2004_09 |