HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → 4-Benzyl-7-methoxy-2,3,4,5-tetrahydro-benzo[f][1,4]oxazepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 22665701 | HCID 22665701 | — |
| Reactant | 4-Benzyl-2,3,4,5-tetrahydrobenzo[f][1,4]oxazepine | HCID 22665902 | — |
| Product | 4-Benzyl-7-methoxy-2,3,4,5-tetrahydro-benzo[f][1,4]oxazepine | HCID 22665706 | — |
Reaction Steps
This compound was prepared from 5.7 g of 4-benzyl-7-methoxy-4,5-dihydro-benzo[f][1,4]-oxazepin-3-one and 2.3 g of lithium aluminum hydride using the procedure described for 64d. Yield: 6.1 g (oil), EI-MS: 269 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06797710B2 |
| Source dataset | uspto-grants-2004_09 |
| ORD ID | ord-a646536d187c4ed9ab2942e0b8123ea0 |
| Source note | uspto-grants-2004_09 |