Nitric Acid → HCID 86615902, compound

HRID 1008928Notes

Reaction equation

HRID 1008928 reaction equation
[C:1]1([CH:7]([CH2:13][S:14]([OH:17])(=[O:16])=[O:15])[CH2:8][S:9]([OH:12])(=[O:11])=[O:10])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.OS(O)(=O)=O.[N+:23]([O-])([OH:25])=[O:24]>>[N+:23]([C:4]1[CH:5]=[CH:6][C:1]([CH:7]([CH2:13][S:14]([OH:17])(=[O:16])=[O:15])[CH2:8][S:9]([OH:12])(=[O:11])=[O:10])=[CH:2][CH:3]=1)([O-:25])=[O:24]

Participants

4

Reactant 3

HCID 944Nitric AcidHCID 1118Sulfuric AcidHCID 86615900HCID 86615900, compound

Product 1

HCID 86615902HCID 86615902, compound

Procedure

2-Phenyl-propane-1,3-disulfonic acid (as prepared in the previous step) is treated with concentrated H2SO4 and fuming HNO3 according to the procedure of Example 2, step (a) to afford the title compound.

Sources & evidence

ORD record
ord-5556c5e82d8149749af7e6061507a16c
Source dataset
uspto-grants-2011_07
Patent number
US07973035B2

Reaction notes

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