HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fumaric Acid → HCID 86595310, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fumaric Acid | HCID 444972 | — |
| Reactant | 2-Chloro-4-(2-(trimethylsilyl)ethynyl)pyridine | HCID 21985391 | — |
| Reactant | 1-(4-fluoro-phenyl)-4-iodo-2-isopropyl-1H-imidazole | HCID 67304175 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86595310 | HCID 86595310 | — |
Reaction Steps
The title compound, MS: m/e=340.1 (M+H+), was prepared in accordance with the general method of example B, step 2, from 2-chloro-4-trimethylsilanylethynyl-pyridine and 1-(4-fluoro-phenyl)-4-iodo-2-isopropyl-1H-imidazole and crystallization from methanol and 1.05 eq fumaric acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07973165B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-1c4b73f5cc474c24b2aa02932c954cd4 |
| Source note | uspto-grants-2011_07 |